SMALL VOLUME LABORATORY ON A CHIP MEASUREMENTS INCORPORATING THE QUARTZ CRYSTAL MICROBALANCE TO MEASURE THE VISCOSITY-DENSITY PRODUCT OF ROOM TEMPERATURE IONIC LIQUIDS
Biomicrofluidics, volume 4, Issue 1, 2010
N. Doy, G. McHale, M. I. Newton, C. Hardacre, R. Ge, J. M. MacInnes, D. Kuvshinov, and R. W. Allen. School of Science and Technology, Nottingham Trent University, Clifton Lane, Nottingham NG11 8NS, United Kingdom
A microfluidic glass chip system incorporating a quartz crystal microbalance (QCM) to measure the square root of the viscosity-density product of room temperature ionic liquids (RTILs) is presented. The QCM covers a central recess on a glass chip, with a seal formed by tightly clamping from above outside the sensing region. The change in resonant frequency of the QCM allows for the determination of the square root viscosity-density product of RTILs to a limit of ∼ 10 kg m−2 s−0.5. This method has reduced the sample size needed for characterization from 1.5 ml to only 30 μl and allows the measurement to be made in an enclosed system.